Effect of moisture and thermocycling on shear bond strength and failure modes of two universal adhesives: an in vitro study
Department of Conservative Dentistry, Faculty of Dentistry, Applied Science Private University, Amman, Jordan
Department of Conservative Dentistry, Al-Azhar University, Assiut Branch, Assiut, Egypt
J Stoma 2026; 79, 3: 190-196
Objectives
In recent years, notable advancements have been made in dental adhesive systems. However, the adhesive interface remains the most vulnerable aspect of tooth-composite restorations. This has created a growing demand for simplified adhesives with enhanced performance, prompting the emergence of universal adhesives.
Material and methods
To evaluate the influence of dentin moisture condition and thermocycling on shear bond strength (SBS), failure modes, and adhesive remnant index (ARI) of two universal adhesives, such as M-TEG-P Yamakin Aquabond (methacryloyloxydecyl tetraethylene glycol phosphate) and MDP One Coat Bond (10-methacryloyloxydecyl dihydrogen phosphate).
Results
Sixty-four extracted maxillary premolars were divided into two main adhesive groups (n = 32 each): Groups 1-4: Yamakin, and groups 5-8: One Coat Bond. Each group was subdivided by moisture condition: dry vs. moist (n = 16 each), and aging condition: immediate vs. thermocycled (n = 8 each). Bonding was performed according to manufacturer instructions, followed by composite build-up. SBS was measured using a universal testing machine, and failure mode was evaluated by XCAM stereomicroscope with ARI. Data were analyzed using ANOVA and Mann-Whitney U tests (a = 0.05).
Conclusions
Statistically significant differences in SBS were observed among the eight subgroups (p < 0.005). The highest SBS was recorded in the One Coat/wet/immediate group (17.2 ± 1.0 MPa), significantly outperforming all other conditions. Thermocycling reduced SBS in both adhesives, with Yamakin groups exhibiting more pronounced degradations. Failure mode analysis revealed a predominance of adhesive failures in Yamakin groups and mixed failures in One Coat groups, aligning with SBS outcomes.
Keywords
shear bond strength, moisture, adhesive remnant index (ARI), thermocycling, universal adhesives, dentin bonding
Integrated with
